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Physical & Chemical properties

Boiling point

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Administrative data

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2016-06-24 to 2016-11-09
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Version / remarks:
27 July 1995
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Version / remarks:
Commission Regulation (EC) No 440/2008 of 30 May 2008
Deviations:
no
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7220 (Boiling Point / Boiling Range)
Version / remarks:
August 1996
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Remarks:
Date of inspection: 05/07/2016; Date of issue: 28/10/2016
Type of method:
differential scanning calorimetry
Key result
Boiling pt.:
271.5 °C
Atm. press.:
102 kPa
Key result
Boiling pt.:
544.6 °C
Atm. press.:
102 kPa

The thermograms and thermographic data for determinations 1 to 4 are shown in Figure 1 to Figure 4 (attached) and in the following table.

Table 1: Thermographic Data

Thermal Event

Interpretation

Temperature

Determination 1

Determination 2

ºC

K

ºC

K

Endotherm

Boiling Onset

271.04

544.2

270.97

544.1

Thermal Event

Interpretation

Temperature

Determination 3

Determination 4

ºC

K

ºC

K

Endotherm

Boiling Onset

271.77

544.9

272.00

545.2

Atmospheric pressure:                      Determination 1 and 2:  101.6 kPa

                                                           Determination 3 and 4:  102.0 kPa

Mean boiling point:                271.5 ± 1.0 °C (544.6 ± 1.0 K) at 102 kPa

Conclusions:
A boiling point value of 271.5 ± 1.0°C (544.6 ± 1.0 K) at 102 kPa was determined for the substance using a relevant test method and in compliance with GLP. The result is considered to be reliable.
Executive summary:

The boiling point of the test item has been determined to be 271.5 ± 1.0 °C (544.6 ± 1.0 K) at 102 kPa.

Description of key information

Boiling point: 271.5 ± 1.0°C (544.6 ± 1.0 K) at 102 kPa (OECD 103)

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
271.5 °C

Additional information

A boiling point temperature value of 271.5 ± 1.0°C (544.6 ± 1.0 K) at 102 kPa was determined for the substance in a Differential Scanning Calorimetry (DSC) study conducted in accordance with OECD Test Guideline 103 and in compliance with GLP. The result is considered to be reliable.