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EC number: 812-877-4 | CAS number: 1228350-17-1
- Life Cycle description
- Uses advised against
- Endpoint summary
- Appearance / physical state / colour
- Melting point / freezing point
- Boiling point
- Density
- Particle size distribution (Granulometry)
- Vapour pressure
- Partition coefficient
- Water solubility
- Solubility in organic solvents / fat solubility
- Surface tension
- Flash point
- Auto flammability
- Flammability
- Explosiveness
- Oxidising properties
- Oxidation reduction potential
- Stability in organic solvents and identity of relevant degradation products
- Storage stability and reactivity towards container material
- Stability: thermal, sunlight, metals
- pH
- Dissociation constant
- Viscosity
- Additional physico-chemical information
- Additional physico-chemical properties of nanomaterials
- Nanomaterial agglomeration / aggregation
- Nanomaterial crystalline phase
- Nanomaterial crystallite and grain size
- Nanomaterial aspect ratio / shape
- Nanomaterial specific surface area
- Nanomaterial Zeta potential
- Nanomaterial surface chemistry
- Nanomaterial dustiness
- Nanomaterial porosity
- Nanomaterial pour density
- Nanomaterial photocatalytic activity
- Nanomaterial radical formation potential
- Nanomaterial catalytic activity
- Endpoint summary
- Stability
- Biodegradation
- Bioaccumulation
- Transport and distribution
- Environmental data
- Additional information on environmental fate and behaviour
- Ecotoxicological Summary
- Aquatic toxicity
- Endpoint summary
- Short-term toxicity to fish
- Long-term toxicity to fish
- Short-term toxicity to aquatic invertebrates
- Long-term toxicity to aquatic invertebrates
- Toxicity to aquatic algae and cyanobacteria
- Toxicity to aquatic plants other than algae
- Toxicity to microorganisms
- Endocrine disrupter testing in aquatic vertebrates – in vivo
- Toxicity to other aquatic organisms
- Sediment toxicity
- Terrestrial toxicity
- Biological effects monitoring
- Biotransformation and kinetics
- Additional ecotoxological information
- Toxicological Summary
- Toxicokinetics, metabolism and distribution
- Acute Toxicity
- Irritation / corrosion
- Sensitisation
- Repeated dose toxicity
- Genetic toxicity
- Carcinogenicity
- Toxicity to reproduction
- Specific investigations
- Exposure related observations in humans
- Toxic effects on livestock and pets
- Additional toxicological data
Water solubility
Administrative data
- Endpoint:
- water solubility
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- September 30-October 19, 2016
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 016
- Report date:
- 2016
Materials and methods
Test guideline
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 105 (Water Solubility)
- Version / remarks:
- adopted July 27, 1995
- Deviations:
- no
- GLP compliance:
- yes (incl. QA statement)
- Type of method:
- column elution method
Test material
- Reference substance name:
- 4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononyl methacrylate
- EC Number:
- 812-877-4
- Cas Number:
- 1228350-17-1
- Molecular formula:
- C13 H11 F13 O2
- IUPAC Name:
- 4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononyl methacrylate
- Test material form:
- liquid
- Details on test material:
- Test Item name Fluowet PMA600
Batch No. DH213/16
Appearance transparent to brownish liquid
Purity 99.4 %
Expiry date 01 June 2017
Storage room temperature, protected from light
Constituent 1
- Specific details on test material used for the study:
- Test Item name Fluowet PMA600
Batch No. DH213/16
Appearance transparent to brownish liquid
Purity 99.4 %
Expiry date 01 June 2017
Storage room temperature, protected from light
Results and discussion
Water solubility
- Key result
- Water solubility:
- 0.076 mg/L
- Conc. based on:
- test mat.
- Loading of aqueous phase:
- 518 mg/L
- Incubation duration:
- 2 h
- Temp.:
- 20 °C
- pH:
- > 6.66 - < 6.68
Any other information on results incl. tables
Results of the determination of Fluowet PMA600 concentrations
Analytical occasion / Time Period hours |
Flow rate (mL/hour) |
Measured concentration ofFluowet PMA600(mg/L) |
||||
Column 1. |
Column 2. |
|||||
October 04, 2016 20; 22 |
~ 25 |
Before the saturation range |
||||
October 07, 2016 88 90 92 94 |
0.103 0.047 0.099 0.104 |
pH = 6.66 pH = 6.67 pH = 6.67 pH = 6.68 |
0.100 0.060 0.076 0083 |
pH = 6.67 pH = 6.68 pH = 6.67 pH = 6.67 |
||
October 09, 2016 142 144.5 147 |
0.099 0.101 0.088 |
pH = 6.67 pH = 6.67 pH = 6.68 |
-* 0.091 0.075 |
pH = 6.66 pH = 6.67 pH = 6.67 |
||
Mean |
0.091 |
pH = 6.67 |
0.081 |
pH = 6.67 |
||
Mean of the Column 1 and Column 2 with95% confidence interval |
0.087 ± 0.011 |
|||||
RSD % |
21 |
|||||
Analytical occasion / Time Period hours |
Flow rate (mL/hour) |
Measured concentration ofFluowet PMA600(mg/L) |
||||
Column 1. |
Column 2. |
|||||
October 10, 201 2.5, 4.5, 10.5 |
~ 15 |
Before the saturation range |
||||
October 11, 2016 26.5 28.5 34 |
0.080 0.056 -* |
pH = 6.68 pH = 6.70 pH = 6.70 |
0.065 0.078 0.064 |
pH = 6.66 pH = 6.67 pH = 6.67 |
||
October 12, 2016 53 55.5 57.5 61 |
0.079 0.069 0.063 0.080 |
pH = 6.80 pH = 6.80 pH = 6.78 pH = 6.80 |
0.073 0.054 0.093 0.078 |
pH = 6.82 pH = 6.84 pH = 6.88 pH = 6.88 |
||
October 13, 2016 75 81 83.5 |
0.078 0.060 0.045 |
pH = 6.82 pH = 6.78 pH = 6.80 |
0.073 0.061 0.053 |
pH = 6.90 pH =6.86 pH = 6.88 |
||
Mean |
0.068 |
pH = 6.77 |
0.069 |
pH = 6.81 |
||
Mean of the Column 1 and Column 2 with95% confidence interval |
0.069 ± 0.006 |
|||||
RSD % |
18 |
|||||
Mean all with 95% confidence interval |
0.076 ±0.006 |
|||||
RSD % |
22 |
|||||
-* Excluded because of a technical error
Applicant's summary and conclusion
- Conclusions:
- In conclusion the water solubility of Fluowet PMA600 was determined to be 0.076 0.006 mg/L (95% confidence interval) at 20 °C ± 1 °C using the column elution method for the performance.
- Executive summary:
The purpose of this study was to determine the solubility of the test item in water at 20±1 °C.
The method is based on the elution of the test substance with water from a micro-column which is charged with an inert support material coated with an excess of test substance. The water solubility is determined when the mass concentration of the eluate is constant. This is shown by a concentration plateau as a function of time.
Results of the test and measured concentrations of Fluowet PMA600 on the two parallel columns using two different flow rates. The measured concentrations are constant within ± 30 % and thus within the range required by the guidelines.
The water solubility of Fluowet PMA600 was determined to be 0.076 ± 0.006 mg/L (95% confidence interval) at± 1 °C using the column elution method for the performance.
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