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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
relative self-ignition temperature (solids)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Experimental Starting Date: 30 October 2012 Experimental Completion Date: 31 October 2012
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: see 'Remark'
Remarks:
Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of the relevant results. The study report was conclusive, done to a valid guideline and the study was conducted under GLP conditions.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2013
Report date:
2013

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.16 (Relative Self-Ignition Temperature for Solids)
Deviations:
no
GLP compliance:
yes

Test material

Constituent 1
Reference substance name:
BMS-528233-01
IUPAC Name:
BMS-528233-01
Details on test material:
Identification: BMS-528233-01
Description: white powder
BMS Batch Number: 2C80150N
Vendor Batch Number: LTBB2S1005
Structure: Please see Attachment 1 of this Summary
Molecular Formula: C17H27NO5
Molecular Weight: 325.41
Purity: 100%
Expiry Date: 31 January 2015
Storage Conditions: room temperature in the dark

Results and discussion

Relative self-ignition temperature (solids)
Remarks on result:
other: The test item has been determined not to have a relative self-ignition temperature below its melting temperature.

Any other information on results incl. tables

The test item was a white powder. Whilst heating the test item,no relevant exothermic reaction of the sample was observed.The temperature curve is shown in Attachment 2 of this Summary. On completion of the test, the cube contained a beige colored hard fused solid.

Applicant's summary and conclusion

Conclusions:
The test item has been determined not to have a relative self-ignition temperature below its melting temperature.
Executive summary:
Testing was conducted using a procedure designed to be compatible with Method A16 Relative Self-Ignition Temperature for Solids of Commission Regulation (EC) No 440/2008 of 30 May 2008.

 

Apparatus:

Oven: A temperature programmed laboratory oven with a Eurotherm temperature controller.

Wire mesh cube:A piece of stainless steel wire mesh with 0.042 mm openings, folded and secured with clips into a cube with dimensions of 2 x 2 x 2 cm.

 

Thermocouples: Type K thermocouples.

 

Recorder: Graphtec GL200a data logger.

 

Conclusion

The test item has been determined not to have a relative self-ignition temperature below its melting temperature.