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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
October 28, 2009
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: Valid method according to company guideline

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2009
Report date:
2009

Materials and methods

Principles of method if other than guideline:
Differential scanning calorimetry (DSC)
Type of method:
thermal analysis
Remarks:
DSC

Test material

Constituent 1
Chemical structure
Reference substance name:
2,2'-[(3,3'-dichloro[1,1'-biphenyl]-4,4'-diyl)bis(azo)]bis[N-(4-ethoxyphenyl)-3-oxobutyramide]
EC Number:
250-799-7
EC Name:
2,2'-[(3,3'-dichloro[1,1'-biphenyl]-4,4'-diyl)bis(azo)]bis[N-(4-ethoxyphenyl)-3-oxobutyramide]
Cas Number:
31775-20-9
Molecular formula:
C36H34Cl2N6O6
IUPAC Name:
2,2'-[(3,3'-dichlorobiphenyl-4,4'-diyl)didiazene-2,1-diyl]bis[N-(4-ethoxyphenyl)-3-oxobutanamide]

Results and discussion

Melting / freezing point
Melting / freezing pt.:
310 °C
Decomposition:
yes
Decomp. temp.:
315 °C

Any other information on results incl. tables

The substance begins to melt at 310°C (taken as melting point). An exothermic decomposition starts at 315°C (taken as decomposition temperature). Because of the overlap of endothermic and exothermic processes, the energy measured for the exothermic process (402 J/g) is less than the true decomposition energy.

Applicant's summary and conclusion

Conclusions:
The test item has a melting point of 310 °C and a decomposition temperature of 350 °C.
Executive summary:
The melting point was determined by DSC to be 310 °C with a decomposition temperature of 315 °C.