Registration Dossier
Registration Dossier
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EC number: 228-787-8 | CAS number: 6358-85-6
Melting point / freezing point
Administrative data
- Endpoint:
- melting point/freezing point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- September 3-25, 1998
- Reliability:
- 2 (reliable with restrictions)
- Rationale for reliability incl. deficiencies:
- guideline study with acceptable restrictions
- Remarks:
- Valid method according to company guideline/standard operating procedure
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 1 998
- Report date:
- 1998
Materials and methods
- Principles of method if other than guideline:
- Differential thermal analysis (DTA)
- Type of method:
- differential scanning calorimetry
- Remarks:
- DTA
Test material
- Reference substance name:
- 2,2'-[(3,3'-dichloro[1,1'-biphenyl]-4,4'-diyl)bis(azo)]bis[3-oxo-N-phenylbutyramide]
- EC Number:
- 228-787-8
- EC Name:
- 2,2'-[(3,3'-dichloro[1,1'-biphenyl]-4,4'-diyl)bis(azo)]bis[3-oxo-N-phenylbutyramide]
- Cas Number:
- 6358-85-6
- Molecular formula:
- C32H26Cl2N6O4
- IUPAC Name:
- 2-[2-(3,3'-dichloro-4'-{2-[2-oxo-1-(phenylcarbamoyl)propyl]diazen-1-yl}-[1,1'-biphenyl]-4-yl)diazen-1-yl]-3-oxo-N-phenylbutanamide
- Test material form:
- solid: nanoform
Constituent 1
Results and discussion
Melting / freezing point
- Melting / freezing pt.:
- 306 °C
- Decomposition:
- yes
- Decomp. temp.:
- 310 °C
Any other information on results incl. tables
The DTA shows an endothermal reaction with an onset at 306.15 °C (rounded value of 306°C taken as melting point) and a peak at 308.03 °C.
Decomposition starts from the melting substance. The (exothermal) decomposition reaction shows an onset at 309.77 °C (rounded value of 310 °C taken as decomposition temperature) and a peak at 318.56 °C, the decomposition energy was -580 J/g (mean from 2 measurements).
Applicant's summary and conclusion
- Executive summary:
The DTA recorded a melting point of 308°C and decomposition from the melting substance at an onset temperature of 310 °C. The decomposition energy is 580 J/g (mean of 2 measurements).
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