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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
From July 14, 2010 to July 21, 2010
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
comparable to guideline study
Qualifier:
equivalent or similar to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Principles of method if other than guideline:
Not applicable
GLP compliance:
not specified
Type of method:
differential scanning calorimetry
Remarks:
Differential Scanning Calorimetry on a Mettler
Key result
Melting / freezing pt.:
ca. -30 - ca. 300 °C
Atm. press.:
ca. 101.3 hPa
Remarks on result:
other: No melting point was detected for the test substance

No obvious melting point was detected for the test substance. The reason for this is probably related to the fact that the substance is paste at room temperature.

Conclusions:
Under the study conditions, no melting point was detected for the test substance because the test substance is a paste at room temperature.
Executive summary:

A study was conducted to determine the melting point of the test substance, C12-18 DAQ (99.6% active), according to the method equivalent or similar to OECD guideline 102.  The analysis was performed with differential scanning calorimetry on a Mettler DSC 1 under nitrogen atmosphere (20 mL/min). The temperature range of -30-300 °C (5 °C/min) was used.12.7 mg of test sample was placed in a 40 µL aluminium cup for analysis. Under the study conditions, no melting point was detected for the test substance because the test substance is a paste at room temperature (Ulama & Karlsson, 2010).

Description of key information

The melting point of the test substance was determined using differential scanning calorimetry (DSC), according to a method similar to OECD Guideline 102 (Ulama, 2010).  

Key value for chemical safety assessment

Additional information

No melting point was detected for the test substance because the test substance is a paste at room temperature.