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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: GLP Guideline Study
Qualifier:
according to guideline
Guideline:
other: OECD 102 / OECD 113
Deviations:
no
Qualifier:
according to guideline
Guideline:
other: EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
other: Differential Thermal Analysis (DTA) / Differential Scanning Calorimetry (DSC)
Boiling pt.:
220 - 290 °C
Atm. press.:
1 atm
Decomposition:
yes
Decomp. temp.:
140 - 215 °C
Remarks on result:
other: No pressure reported

From room temperature to 450 °C no definite boiling point could be observed. The inconstant endothermic effects between 220 °C and 290 °C could be interpreted as boiling range around 250 °C, very probably under degradation of the sample indicated by the unsteady base line.

Conclusions:
From room temperature up to 450 °C no definite boiling point could be observed. The inconstant endothermic effects between 220 °C and 290 °C could be interpreted as boiling range around 250 °C. After the heating process a brownish residue remained in the crucible which indicates decomposition.
Executive summary:

According to EU Method A. 1 no definite boiling point was detected. Between approx. 220 and approx. 290 °C a range of inconstant endothermic effects were detected. The inconstant endothermic effects could be interpreted as boiling range around 250 °C, very probably under degradation of the sample indicated by the unsteady base line. From approx. 330 °C up to approx. 450 °C a further exothermic effect was visible. After the heating process a brownish residue remained in the crucible which indicates decomposition of the test item.

Description of key information

Endothermic effects between 220 °C and 290 °C could be interpreted as a boiling range around 250 °C. 

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
250 °C

Additional information

From room temperature up to 450 °C no definite boiling point could be observed. The inconstant endothermic effects between 220 °C and 290 °C could be interpreted as boiling range around 250 °C. After the heating process a brownish residue remained in the crucible which indicates decomposition.