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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2011-09-28
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: study performed in a laboratory holding a GLP statement

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2011
Report date:
2011

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes
Type of method:
other: photocell method

Test material

Constituent 1
Reference substance name:
LCE11051
IUPAC Name:
LCE11051
Details on test material:
- Name of test material (as cited in study report):LCE11051 acetalization product between glucose and C12/18(even numbered) alcohol
- Substance type:UVCB
- Physical state:solid
- Analytical purity:100%
- Lot/batch No.:T12825

Results and discussion

Melting / freezing point
Melting / freezing pt.:
57 °C
Remarks on result:
other: the test substanec was a cream waxy pellet and was ground to give a fine powder before analysis

Applicant's summary and conclusion

Conclusions:
. The Melting point average, of this test, to be reported is 57°C
Executive summary:

A melting point tube was filed in triplicate with test substance. The test substance was a cream waxy pellet and was ground to give a fine powder before analysis

 

Using a preliminary temperature gradient of 25°C to 300°C at 5°C/min , analysed in triplicate, gave approximate results of 56.0°C,61.3°C and 56.7°C, average value of 57°C.

Using a slower temperature gradient oft 53°C to 63°C at a rate of 0.5°C/min to increase accuracy, the tests substance, analysed in triplicate, gave results of 57.1°C,57.0°C and 56.8°C. The Melting point average, of this test, to be reported is 57°C