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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
23 September - 29 December 2015
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2016
Report date:
2016

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7220 (Boiling Point / Boiling Range)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
3-(2-CHLOROETHYL)-9-HYDROXY-2-METHYL-4H-PYRIDO[1,2-A]PYRIMIDIN-4-ONE HYDROCHLORIDE (1:1)
EC Number:
617-648-0
Cas Number:
849727-62-4
Molecular formula:
C11H11ClN2O2.HCl
IUPAC Name:
3-(2-CHLOROETHYL)-9-HYDROXY-2-METHYL-4H-PYRIDO[1,2-A]PYRIMIDIN-4-ONE HYDROCHLORIDE (1:1)
Test material form:
solid: particulate/powder
Specific details on test material used for the study:
- Batch n°: I15BB0722
- Expiration date: 21 February 2017
- Storage condition: at room temperature

Results and discussion

Boiling point
Key result
Atm. press.:
1 013.25 hPa
Decomposition:
yes
Decomp. temp.:
> 224.9 °C
Remarks on result:
other: Boiling of the test item was not observed below the temperature of decomposition and/or reaction, therefore the test item has no boiling temperature.

Any other information on results incl. tables

Boiling of the test item was not observed below the temperature of decomposition and/or reaction. Based on this, the test item has no boiling temperature.

Applicant's summary and conclusion

Conclusions:
Reaction and/or decomposition of JNJ-1692405-AAC (T002006) was observed during DSC experiments during and directly after melting. Boiling of the test item was not observed below the temperature at which reaction and/or decomposition started. Based on this, the test item has no boiling temperature.