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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
17.07.2018 - 19.07.2018
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
adopted by the Council on 27th July 1995
Deviations:
no
GLP compliance:
no
Other quality assurance:
ISO/IEC 17025 (General requirements for the competence of testing and calibration laboratories)
Type of method:
differential scanning calorimetry
Key result
Melting / freezing pt.:
88 - 101 °C

To determine the melting behaviour (three independent single measurements), the test item was measured by DSC between -90 °C and 150 °C with a heating / cooling rate of 10 K/min in 3 cycles. For the measurement a capsulated crucible was used.

The test item MCC-5424/18 shows a melting area of crystalline main components between 88 °C and 101 °C according to the definition in the OECD Guideline 102 (mean value from repeat determination). Additional the test item shows a melting of a sub component at 34 °C.

Melting of main component (2nd heating run)

88 °C and 102 °C (from first measurement)

88 °C and 101 °C (from second measurement)

88 °C and 101 °C (from third measurement)

The cooling runs show crystallization.

Conclusions:
The test item MCC-5424/18 shows a melting area of crystalline subcomponents between 88 °C and 101 °C according to the definition in the OECD Guideline 102 (mean value from repeat determination).

Description of key information

The test item MCC-5424/18 shows a melting area of crystalline subcomponents between 88 °C and 101 °C according to the definition in the OECD Guideline 102 (mean value from repeat determination).

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
88 °C

Additional information