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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
10 September 2010 – 02 November 2010
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: This study has been performed according to OECD and EC guidelines and according to GLP principles.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2010
Report date:
2010

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Reference substance name:
No.476 YELLOW
IUPAC Name:
No.476 YELLOW
Details on test material:
- Substance type: Yellow to orange powder (determined at NOTOX)
- Lot/batch No.: 00082

Results and discussion

Boiling point
Decomposition:
yes
Decomp. temp.:
> 225 °C
Remarks on result:
other: no boiling of the test substance was observed below 225°C; substance has no boiling temperature

Any other information on results incl. tables

Preliminary test

From 250°C upwards the weight of the sample decreased significantly. At 347°C the sample weight had decreased by 25%. After the experiment, black residue was observed on the lid of the sample container and a charred residue remained in the sample container (original colour: yellow to orange). The change of the colour indicated reaction and/or decomposition of the test substance.

 

Main study

No effects were observed which were due to melting and/or boiling of the test substance. Exothermic effects starting at 225°C were indicating reaction and/or decomposition of the test substance. After the experiment, black residue was observed on the lid of the sample container and a charred residue remained in the sample container (original colour: yellow to orange). The change of the colour indicated reaction and/or decomposition of the test substance.

Applicant's summary and conclusion

Conclusions:
Reaction and/or decomposition of the test substance was observed starting at 225°C (498K). Boiling of the test substance was not observed below this temperature. Based on this, the test substance has no boiling temperature.