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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
October 18, 2012 - October 19, 2012.
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Remarks:
Test method in accordance with EU Method A.1 and OECD Guideline 102. GLP study.
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
method to determine freezing temperature
Remarks:
(PN-ISO 1392:2002)
Key result
Melting / freezing pt.:
< -30 °C
Remarks on result:
other: see the comments on "any other information on results incl. tables"

No crystals evidence have been noticed in all measurements. According to Guidance on information requirements and chemical safety assessment Chapter R.7a: Endpoint specific guidance, May 2008, Guidance for the implementation of REACH the study does not need to be conducted below the determination lower limit of -20 °C. The freezing point was determined to be below of -30 °C.

Conclusions:
The freezing point of the test substance was determined to be < -30 ºC.
Executive summary:

A freezing point determination test was performed in accordance with EU Method A.1 and OECD Guideline 102 (PN-ISO 1392:2002). The freezing point of the test substance was determined to be lower than -30 ºC since no crystal evidence were noticed in all three measurements.

Description of key information

Key study: EU Method A.1 and OECD Guideline 102. GLP study. The freezing point was determined to be < -30 ºC.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-30 °C

Additional information

Key study: A freezing point determination test was performed in accordance with EU Method A.1 and OECD Guideline 102 (PN-ISO 1392:2002). GLP study. The freezing point of the test substance was determined to be lower than -30 ºC.