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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
20 February 2008 to 28 February 2008
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
test procedure in accordance with generally accepted scientific standards and described in sufficient detail

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2008
Report date:
2008

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
other: differential scanning calorimetry (DSC)

Test material

Constituent 1
Chemical structure
Reference substance name:
diethyl(triethoxysilyl)amine
EC Number:
700-051-5
Cas Number:
35077-00-0
Molecular formula:
C10H25NO3Si
IUPAC Name:
diethyl(triethoxysilyl)amine

Results and discussion

Melting / freezing point
Melting / freezing pt.:
< 253 K

Any other information on results incl. tables

Thermographic data for Determinations 1 and 2 are shown in the following tables respectively:

Table 1:       Thermographic Data - Determination 1

Thermal Event

Interpretation

Temperature

ºC

K

no events

melting/freezing temperature

-20.0

253

Table 2:       Thermographic Data - Determination 2

Thermal Event

Interpretation

Temperature

ºC

K

no events

melting/freezing temperature

-20.0

253

Please see Attachment 1 for Thermogram data.

Applicant's summary and conclusion

Conclusions:
The melting/freezing temperature of the test material has been determined to be less than 253 ± 0.5 K.
Executive summary:

The determination was carried out by differential scanning calorimetry (DSC) using the procedure specified in ASTM E537-86, Method A1 of Commission Directive 92/69/EEC (which constitutes Annex V of Council Directive 67/548/EEC).

The melting/freezing temperature of the test material has been determined to be less than 253 ± 0.5 K.