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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
nanomaterial porosity
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
test procedure in accordance with national standard methods
Cross-referenceopen allclose all
Reason / purpose for cross-reference:
reference to same study
Reference
Endpoint:
nanomaterial specific surface area
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
test procedure in accordance with national standard methods
Reason / purpose for cross-reference:
reference to same study
Qualifier:
according to guideline
Guideline:
ISO 9277 Determination of the specific surface area of solids by gas adsorption - BET method
GLP compliance:
no
Type of method:
BET
Specific details on test material used for the study:
form: High surface area alumina (nanofrom)
Instruments:
QUANTACHROME NOVA 3000e
Specific Surface Area:
208 m²/g

Slope = 16.583

Intercept = 2.000e-01

Correlation coefficient, r = 0.999990

C constant = 83.918

Surface Area = 207.505 m²/g

Reason / purpose for cross-reference:
reference to same study
Reference
Endpoint:
density, other
Remarks:
true density
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
test procedure in accordance with national standard methods
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Qualifier:
according to guideline
Guideline:
other: DIN 66137-2 True density by He-Pycnometry
GLP compliance:
no
Type of method:
pycnometer method
Remarks:
He pycnometry
Specific details on test material used for the study:
Samples have been dried for 3.5 h at 105 °C and cooled down in an exsiccator before measurement.
Type:
other: true density
Density:
3.092 g/cm³
Temp.:
24.02 °C
Remarks on result:
other: Density Std. Dev.: 0.0009 g/cm³

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2015
Report date:
2015

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
other: DIN 66133
Version / remarks:
Mercury Porosimetry
Qualifier:
according to guideline
Guideline:
other: DIN 66137-2
Version / remarks:
True Density by He-Pycnometry
GLP compliance:
no
Type of method:
other: Mercury Porosimetry, He-Pycnometry

Test material

Constituent 1
Chemical structure
Reference substance name:
Aluminium oxide
EC Number:
215-691-6
EC Name:
Aluminium oxide
Cas Number:
1344-28-1
Molecular formula:
Al2O3
IUPAC Name:
oxo[(oxoalumanyl)oxy]alumane
Test material form:
solid: nanoform

Data gathering

Instruments:
POREMASTER 60G

Results and discussion

Porosity (fraction of void space in the material)
Mean:
60 %
Specific pore volume
Mean:
0.493 cm³/g
Modal pore diameter
Mean:
8 nm

Any other information on results incl. tables

Additionally the true density was determined with a QUANTACHROME Ultrapycnometer 1200e (Helium) was determined to be 3.092 g/cm³

Applicant's summary and conclusion