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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
1996-03-21 to 1996-07-19
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
1996
Report date:
1996

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Deviations:
no
Qualifier:
according to guideline
Guideline:
other: OJEC L383 A/15-21
Deviations:
no
GLP compliance:
yes
Type of method:
method according to Siwoloboff

Test material

Constituent 1
Chemical structure
Reference substance name:
-
EC Number:
421-300-1
EC Name:
-
Cas Number:
138564-59-7
Molecular formula:
C12H9N3O2S
IUPAC Name:
5-methyl-2-[(2-nitrophenyl)amino]thiophene-3-carbonitrile
Test material form:
solid: particulate/powder
Details on test material:
97.7%
Item code QA405K
Lilly lot no: 356MO1
Specific details on test material used for the study:
SOURCE OF TEST MATERIAL
- Source and lot/batch No.of test material: Sponsor and 356M01
- Expiration date of the lot/batch: 1997-01-04

STABILITY AND STORAGE CONDITIONS OF TEST MATERIAL
- Storage condition of test material: At ambient temperature in the dark.

Results and discussion

Boiling point
Key result
Atm. press.:
ca. 1 atm
Decomposition:
yes
Decomp. temp.:
ca. 101 °C
Remarks on result:
not determinable
Remarks:
Decomposition prevented the accurate ascertation of the boiling temperature.

Applicant's summary and conclusion

Conclusions:
The boiling point of the test substance was unable to be determined according to guideline due to decomposition prior to the boiling point.
Executive summary:

The boiling point of this test substance was carried out in accordance with OECD Guideline 103, however, it could not be determined due to decomposition prior to the boiling point.