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Physical & Chemical properties

Boiling point

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2018-02-16
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to
Guideline:
OECD Guideline 103 (Boiling Point)
Deviations:
no
Qualifier:
according to
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
GLP compliance:
yes (incl. certificate)
Type of method:
method according to Siwoloboff
Specific details on test material used for the study:
- Batch No.of test material: 20141015
- Purity: 99.35%
- Expiration date of the lot/batch: January 2019
- Stability under test conditions: Room temperature
Key result
Boiling pt.:
244.4 °C
Decomposition:
no
Remarks on result:
other: Corrected due to barometric pressure

Full test results:

Run Number

Mass of sample Used

 

Boiling Temperature

 

(g)

 

(°C)

1

0.11

 

245.0

2

0.18

 

244.8

Mean Boiling Temp (°C)

 

244.9

 

- Mean boiling temperature at a pressure of 102.4 kPa: 244.9 °C

- Boiling temperature corrected due to barometric pressure: 244.4 °C

Conclusions:
The boiling point of the test item has been determined to be 244.4 °C.

Description of key information

A GLP-compliant study was performed according to OECD guideline 103 and EU Method A.2. The boiling point of the test substance was found to be 244.4 °C (K1, Dekra, 2018).

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
244.4 °C

Additional information