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Diss Factsheets

Administrative data

Endpoint:
relative self-ignition temperature (solids)
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2012

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.16 (Relative Self-Ignition Temperature for Solids)
GLP compliance:
yes (incl. QA statement)

Test material

Constituent 1
Chemical structure
Reference substance name:
3,4-diaminobenzenesulphonic acid
EC Number:
231-274-1
EC Name:
3,4-diaminobenzenesulphonic acid
Cas Number:
7474-78-4
Molecular formula:
C6H8N2O3S
IUPAC Name:
3,4-diaminobenzene-1-sulfonic acid
Details on test material:
Chemical Name (IUPAC): 3,4-diaminobenzenesulfonic acid
Molecular Formula: C6H8N2O3S
CAS-No.: 7474-78-4
Molecular Weight: 188.205 g/mol
Batch No.: N-18326
Purity: 99.8 [%, w/w]
Date of expiry: 15.09.2013
Certificate of analysis: No AZ-009-2011, 11.10.2011

Results and discussion

Relative self-ignition temperature (solids)
Relative self-ignition temperature:
>= 342 °C
Remarks on result:
other:

Any other information on results incl. tables

There was no self heating observed up to the melting point of the test item (287°C).

However a self-ignition temperature of 342°C (615 K) was found after the melting point of the test item. This was possible, because the sample did not dropped completely through the mesh wire of the cube. For details refer to the temperatur / time-curve in this report.

The test item 3,4-diaminobenzenesulfonic acid is not self-ignitable up to the melting point at 287°C according to the EC-Guideline A.16.

A self-ignition temperature of 342°C was found after the melting point of the test item.

Applicant's summary and conclusion