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Boiling point

Link to relevant study record(s)

Reference

Endpoint:

boiling point

Type of information:

experimental study

Adequacy of study:

key study

Reliability:

2 (reliable with restrictions)

Rationale for reliability incl. deficiencies:

guideline study with acceptable restrictions

Qualifier:

according to guideline

Guideline:

OECD Guideline 103 (Boiling Point)

GLP compliance:

yes

Type of method:

method according to Siwoloboff

Specific details on test material used for the study:

Test Item Name TYZOR AC 436
IUPAC Name Citric acid, titanium salt
C.A. Name Information not provided by Sponsor
CAS Number (EC # 923-927-0)
Batch/Lot Number 334-301300/000005
Analysed Purity As Ti: 4.9% w/w (Refer Certificate of Analysis in APPENDIX 2)
Appearance Yellow to brownish clear liquid
Manufactured by Dorf Ketal Speciality Catalyst Private Limited
Supplied to JRF by Dorf Ketal Speciality Catalyst Private Limited
Date of Manufacture September 2017
Date of Expiry September 2019
Storage Condition (at JRF) As per the instruction received from the Sponsor on storage of the test item, the test was stored:
Storage Condition : Protected from light, air and moisture. Once opened container was kept under nitrogen blanket to prevent composition .

Key result

Boiling pt.:

ca. 126.27 °C

Atm. press.:

ca. 760 mm Hg

The boiling point/boiling rangeof TYZOR AC 436 was determined using Siwoloboff method.

The boiling point of TYZOR AC 436 was 399.55, 399.55and 399.45K at normal atmospheric pressure (760 mm Hg).

The mean boiling point of TYZOR AC 436 was 399.52± 0.06K (126.37 ± 0.06°C) at normal atmospheric pressure (760 mm Hg) [TABLE 1].

The boiling point of TYZOR AC 436 was 119.60-122.80 °C at normal atmospheric pressure (760 mm Hg) [TABLE 1].

TABLE1:Boiling Point/Boiling RangeValues ofTYZOR AC 436

Atmospheric Pressure 760 mmHg
Repli-cation	Temperature of Initiation of Bubble Formation (°C)	Temperature at which Continuous String of Bubbles were Observed (°C)	Boiling Point Range	Boiling Point
				(°C)	Kelvin (K)
R1	119.60	122.80	119.60-122.80	126.40	399.55
R2	119.80	122.70		126.40	399.55
R3	119.60	122.80		126.30	399.45
Mean				126.37	399.52
Standard Deviation				0.06	0.06
Typical Calculation
Boiling Point [in Kelvin (K)]=Observed Boiling Point(°C) + 273.15                                           =126.40 + 273.15                                           = 399.55

Conclusions:

The mean boiling point of the TYZOR AC 436 was observed by Siwoloboff method and was found to be 126.37 °C at normal atmospheric pressure i.e. 760 mm Hg.

Executive summary:

The mean boiling point of the TYZOR AC 436 was observed by Siwoloboff method and was found to be 126.37 °C at normal atmospheric pressure i.e. 760 mm Hg.

Description of key information

The flash point of TYZOR AC 436 was determined by the Pensky MartensClosed TesterMethod and it was found to be> 105 °C at normal atmospheric pressure 760 mm Hg